Jakob, Cordula ; Jansen, Daniel ; Ukrainczyk, Neven ; Koenders, Eddie ; Pott, Ursula ; Stephan, Dietmar ; Neubauer, Jürgen (2024)
Relating Ettringite Formation and Rheological Changes during the Initial Cement Hydration: A Comparative Study Applying XRD Analysis, Rheological Measurements and Modeling.
In: Materials, 2019, 12 (18)
doi: 10.26083/tuprints-00016232
Artikel, Zweitveröffentlichung, Verlagsversion
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Kurzbeschreibung (Abstract)
In order to gain a deeper understanding of the rheological development of hydrating ordinary Portland cement (OPC) pastes at initial state, and to better understand their underlying processes, quantitative X-ray diffraction (XRD) analysis and rheological measurements were conducted and their results combined. The time-dependent relation between phase development and flow behavior of cement paste was investigated at two different temperatures (20 and 30 °C), over a period of two hours. Regarding the phase development during hydration, ettringite precipitation was identified as the dominant reaction in the first two hours. For both temperatures, the increasing ettringite content turned out to correlate very well with the loss of workability of the reacting cement paste. An exponential relationship between ettringite growth and flow behavior was observed that could be explained by applying the Krieger-Dougherty equation, which describes the influence of solid fraction on the viscosity of a suspension.
| Typ des Eintrags: | Artikel |
|---|---|
| Erschienen: | 2024 |
| Autor(en): | Jakob, Cordula ; Jansen, Daniel ; Ukrainczyk, Neven ; Koenders, Eddie ; Pott, Ursula ; Stephan, Dietmar ; Neubauer, Jürgen |
| Art des Eintrags: | Zweitveröffentlichung |
| Titel: | Relating Ettringite Formation and Rheological Changes during the Initial Cement Hydration: A Comparative Study Applying XRD Analysis, Rheological Measurements and Modeling |
| Sprache: | Englisch |
| Publikationsjahr: | 16 Januar 2024 |
| Ort: | Darmstadt |
| Publikationsdatum der Erstveröffentlichung: | 2019 |
| Ort der Erstveröffentlichung: | Basel |
| Verlag: | MDPI |
| Titel der Zeitschrift, Zeitung oder Schriftenreihe: | Materials |
| Jahrgang/Volume einer Zeitschrift: | 12 |
| (Heft-)Nummer: | 18 |
| Kollation: | 12 Seiten |
| DOI: | 10.26083/tuprints-00016232 |
| URL / URN: | https://tuprints.ulb.tu-darmstadt.de/16232 |
| Zugehörige Links: | |
| Herkunft: | Zweitveröffentlichung DeepGreen |
| Kurzbeschreibung (Abstract): | In order to gain a deeper understanding of the rheological development of hydrating ordinary Portland cement (OPC) pastes at initial state, and to better understand their underlying processes, quantitative X-ray diffraction (XRD) analysis and rheological measurements were conducted and their results combined. The time-dependent relation between phase development and flow behavior of cement paste was investigated at two different temperatures (20 and 30 °C), over a period of two hours. Regarding the phase development during hydration, ettringite precipitation was identified as the dominant reaction in the first two hours. For both temperatures, the increasing ettringite content turned out to correlate very well with the loss of workability of the reacting cement paste. An exponential relationship between ettringite growth and flow behavior was observed that could be explained by applying the Krieger-Dougherty equation, which describes the influence of solid fraction on the viscosity of a suspension. |
| Freie Schlagworte: | hydration kinetics, rheology, ettringite formation, OPC, temperature, modeling, scanning electron microscopy (SEM) |
| Status: | Verlagsversion |
| URN: | urn:nbn:de:tuda-tuprints-162328 |
| Zusätzliche Informationen: | This article belongs to the Special Issue Modeling of Cementitious Materials and Structures |
| Sachgruppe der Dewey Dezimalklassifikatin (DDC): | 600 Technik, Medizin, angewandte Wissenschaften > 624 Ingenieurbau und Umwelttechnik |
| Fachbereich(e)/-gebiet(e): | 13 Fachbereich Bau- und Umweltingenieurwissenschaften 13 Fachbereich Bau- und Umweltingenieurwissenschaften > Institut für Werkstoffe im Bauwesen |
| Hinterlegungsdatum: | 16 Jan 2024 12:15 |
| Letzte Änderung: | 17 Jan 2024 14:32 |
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| Suche nach Titel in: | TUfind oder in Google |
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- Relating Ettringite Formation and Rheological Changes during the Initial Cement Hydration: A Comparative Study Applying XRD Analysis, Rheological Measurements and Modeling. (deposited 16 Jan 2024 12:15) [Gegenwärtig angezeigt]
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