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Indentation size effectin tungsten: Quantification of geometrically necessary dislocations underneath the indentations using HR-EBSD

Javaid, Farhan ; Xu, Y. ; Bruder, Enrico ; Durst, Karsten (2018)
Indentation size effectin tungsten: Quantification of geometrically necessary dislocations underneath the indentations using HR-EBSD.
In: Materials Characterization, (142)
doi: 10.1016/j.matchar.2018.05.016
Artikel, Bibliographie

Kurzbeschreibung (Abstract)

During indentation testing of the low defect density crystalline materials, higher hardness values are found at lower indentation depths, which is referred to as an indentation size effect. The depth-dependence of hardness can be described by the Nix-Gao model, which is based on the concept of Geometrically Necessary Dislocations (GNDs). The underlying dislocation mechanism remains, however, unclear and requires independent measurement of GND density below the indentation. In the present work, the depth-dependency of the GND density is quantified underneath the Berkovich indentations in tungsten via high-resolution electron backscatter diffraction. There a higher GND density is found for lower indentation depths, resulting in a higher Taylor hardness for measured GND density.

Typ des Eintrags: Artikel
Erschienen: 2018
Autor(en): Javaid, Farhan ; Xu, Y. ; Bruder, Enrico ; Durst, Karsten
Art des Eintrags: Bibliographie
Titel: Indentation size effectin tungsten: Quantification of geometrically necessary dislocations underneath the indentations using HR-EBSD
Sprache: Englisch
Publikationsjahr: August 2018
Verlag: ELSEVIER SCIENCE INC, USA
Titel der Zeitschrift, Zeitung oder Schriftenreihe: Materials Characterization
(Heft-)Nummer: 142
DOI: 10.1016/j.matchar.2018.05.016
Kurzbeschreibung (Abstract):

During indentation testing of the low defect density crystalline materials, higher hardness values are found at lower indentation depths, which is referred to as an indentation size effect. The depth-dependence of hardness can be described by the Nix-Gao model, which is based on the concept of Geometrically Necessary Dislocations (GNDs). The underlying dislocation mechanism remains, however, unclear and requires independent measurement of GND density below the indentation. In the present work, the depth-dependency of the GND density is quantified underneath the Berkovich indentations in tungsten via high-resolution electron backscatter diffraction. There a higher GND density is found for lower indentation depths, resulting in a higher Taylor hardness for measured GND density.

Freie Schlagworte: Tungsten, Indentation size effect, Geometrically necessary dislocations, HR-EBSD, ECCI
Fachbereich(e)/-gebiet(e): 11 Fachbereich Material- und Geowissenschaften
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Physikalische Metallkunde
Hinterlegungsdatum: 29 Mai 2018 10:41
Letzte Änderung: 17 Jul 2018 12:13
PPN:
Sponsoren: The authors would like to thank Dr. Graham Meaden and Dr. David Dingley from BLG Vantage for Crosscourt software support.
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