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Synthesis of monodisperse spherical silicondicarbodiimide particles

Li, Y.-L. ; Kroke, E. ; Klonczynski, A. ; Riedel, R. (2000)
Synthesis of monodisperse spherical silicondicarbodiimide particles.
In: Advanced materials, 12 (13)
Article, Bibliographie

Abstract

Spherical particles of silicon dicarbodiimide (SiC2N4, see Figure) are synthesized here via the reaction of tetrachlorosilane (T) and bis (trimethylsilyl)carbodiimide (B) using pyridine as a catalyst and toluene or tetrahydrofuran as solvent. It is shown that the morphology of the thus obtained monodisperse particles strongly depends on the molar ratio of the reagents and the type and amount of solvent used.

Item Type: Article
Erschienen: 2000
Creators: Li, Y.-L. ; Kroke, E. ; Klonczynski, A. ; Riedel, R.
Type of entry: Bibliographie
Title: Synthesis of monodisperse spherical silicondicarbodiimide particles
Language: English
Date: June 2000
Publisher: Wiley
Journal or Publication Title: Advanced materials
Volume of the journal: 12
Issue Number: 13
Abstract:

Spherical particles of silicon dicarbodiimide (SiC2N4, see Figure) are synthesized here via the reaction of tetrachlorosilane (T) and bis (trimethylsilyl)carbodiimide (B) using pyridine as a catalyst and toluene or tetrahydrofuran as solvent. It is shown that the morphology of the thus obtained monodisperse particles strongly depends on the molar ratio of the reagents and the type and amount of solvent used.

Uncontrolled Keywords: Carbodiimides, Colloids;Silicon, Silicon dicarbodiimide
Divisions: 11 Department of Materials and Earth Sciences
11 Department of Materials and Earth Sciences > Material Science
11 Department of Materials and Earth Sciences > Material Science > Dispersive Solids
Date Deposited: 19 Nov 2008 15:57
Last Modified: 20 Feb 2020 13:27
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Funders: The authors gratefully acknowledge the Deutsche Forschungsgemeinschaft (DFG), Bonn (Germany), for financial support of the present work. Y.-L. Li thanks the Alexander von Humboldt Foundation for a research fellowship.
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