Li, Y.-L. ; Kroke, E. ; Klonczynski, A. ; Riedel, R. (2000):
Synthesis of monodisperse spherical silicondicarbodiimide particles.
In: Advanced materials, 12 (13), pp. 956-961. Wiley, [Article]
Abstract
Spherical particles of silicon dicarbodiimide (SiC2N4, see Figure) are synthesized here via the reaction of tetrachlorosilane (T) and bis (trimethylsilyl)carbodiimide (B) using pyridine as a catalyst and toluene or tetrahydrofuran as solvent. It is shown that the morphology of the thus obtained monodisperse particles strongly depends on the molar ratio of the reagents and the type and amount of solvent used.
| Item Type: | Article |
|---|---|
| Erschienen: | 2000 |
| Creators: | Li, Y.-L. ; Kroke, E. ; Klonczynski, A. ; Riedel, R. |
| Title: | Synthesis of monodisperse spherical silicondicarbodiimide particles |
| Language: | English |
| Abstract: | Spherical particles of silicon dicarbodiimide (SiC2N4, see Figure) are synthesized here via the reaction of tetrachlorosilane (T) and bis (trimethylsilyl)carbodiimide (B) using pyridine as a catalyst and toluene or tetrahydrofuran as solvent. It is shown that the morphology of the thus obtained monodisperse particles strongly depends on the molar ratio of the reagents and the type and amount of solvent used. |
| Journal or Publication Title: | Advanced materials |
| Volume of the journal: | 12 |
| Issue Number: | 13 |
| Publisher: | Wiley |
| Uncontrolled Keywords: | Carbodiimides, Colloids;Silicon, Silicon dicarbodiimide |
| Divisions: | 11 Department of Materials and Earth Sciences 11 Department of Materials and Earth Sciences > Material Science 11 Department of Materials and Earth Sciences > Material Science > Dispersive Solids |
| Date Deposited: | 19 Nov 2008 15:57 |
| PPN: | |
| Funders: | The authors gratefully acknowledge the Deutsche Forschungsgemeinschaft (DFG), Bonn (Germany), for financial support of the present work. Y.-L. Li thanks the Alexander von Humboldt Foundation for a research fellowship. |
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