Hamm, Christin M. ; Diop, Léopold V. B. ; Zhang, Hogbin ; Gutfleisch, Oliver ; Birkel, Christina S. (2017)
Microwave synthesis and magnetic properties of Laves-type Ti2M3Si (M = Mn, Fe, Co, Ni).
In: physica status solidi (c), 14 (3-4)
doi: 10.1002/pssc.201700027
Artikel, Bibliographie
Kurzbeschreibung (Abstract)
Fast and energy-efficient synthesis methods become increasingly important aspects in the experimental high throughput searching of functional materials. Particularly high-temperature solid-state preparation techniques typically require large amounts of energy due to extended heating cycles. Therefore, we have utilized a time and energy-efficient synthesis method using a commercial microwave oven in order to prepare intermetallic Laves-type phases. Ti2M3Si with M = Mn, Fe, Co, Ni can be prepared within only 10 min of microwave heating based on this convenient one-step procedure. These compounds are of interest because of their potentially useful magnetic properties and therefore contribute to the ongoing search for rare earth-free alternatives to state-of-the-art magnetic materials.Transition metal-based Laves phase compounds Ti2M3Si were prepared by time- and energy-efficient microwave heating and their structural and magnetic properties studied.
| Typ des Eintrags: | Artikel |
|---|---|
| Erschienen: | 2017 |
| Autor(en): | Hamm, Christin M. ; Diop, Léopold V. B. ; Zhang, Hogbin ; Gutfleisch, Oliver ; Birkel, Christina S. |
| Art des Eintrags: | Bibliographie |
| Titel: | Microwave synthesis and magnetic properties of Laves-type Ti2M3Si (M = Mn, Fe, Co, Ni) |
| Sprache: | Englisch |
| Publikationsjahr: | 27 Juli 2017 |
| Titel der Zeitschrift, Zeitung oder Schriftenreihe: | physica status solidi (c) |
| Jahrgang/Volume einer Zeitschrift: | 14 |
| (Heft-)Nummer: | 3-4 |
| DOI: | 10.1002/pssc.201700027 |
| Kurzbeschreibung (Abstract): | Fast and energy-efficient synthesis methods become increasingly important aspects in the experimental high throughput searching of functional materials. Particularly high-temperature solid-state preparation techniques typically require large amounts of energy due to extended heating cycles. Therefore, we have utilized a time and energy-efficient synthesis method using a commercial microwave oven in order to prepare intermetallic Laves-type phases. Ti2M3Si with M = Mn, Fe, Co, Ni can be prepared within only 10 min of microwave heating based on this convenient one-step procedure. These compounds are of interest because of their potentially useful magnetic properties and therefore contribute to the ongoing search for rare earth-free alternatives to state-of-the-art magnetic materials.Transition metal-based Laves phase compounds Ti2M3Si were prepared by time- and energy-efficient microwave heating and their structural and magnetic properties studied. |
| Fachbereich(e)/-gebiet(e): | 11 Fachbereich Material- und Geowissenschaften 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Funktionale Materialien 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Theorie magnetischer Materialien 07 Fachbereich Chemie 07 Fachbereich Chemie > Eduard Zintl-Institut > Fachgebiet Anorganische Chemie |
| Hinterlegungsdatum: | 27 Jul 2017 09:22 |
| Letzte Änderung: | 01 Feb 2023 07:46 |
| PPN: | |
| Sponsoren: | Financial support by the DFG (BI1775/2-1) and the German federal state of Hessen through its excellence program LOEWE “RESPONSE“ is gratefully acknowledged. |
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