Mojić-Lanté, Bojana ; Djenadic, Ruzica ; Chakravadhanula, Venkata Sai Kiran ; Kübel, Christian ; Srdić, Vladimir V. ; Hahn, Horst ; Mullins, W. (2015)
Chemical Vapor Synthesis of FeOx-BaTiO3Nanocomposites.
In: Journal of the American Ceramic Society, 98 (6)
doi: 10.1111/jace.13531
Artikel, Bibliographie
Kurzbeschreibung (Abstract)
Nanocomposite powders of FeOx-BaTiO3 (FO-BTO) have been prepared by chemical vapor synthesis (CVS) in a single-step process. The optimal parameters (reactor temperature, reactor length, precursor ratio) for the synthesis were investigated in an initial step for the individual systems, iron oxide (FO), and barium titanate (BTO); and in a second step optimized for the synthesis of the nanocomposites. The solid iron precursor was thermally evaporated, whereas the solid Ba- and Ti precursors were vaporized using laser flash evaporation to obtain ultrafine crystalline FO, BTO, and FO-BTO nanoparticles. The possibility to influence the mass ratios of the two phases in FO-BTO mixture by adjusting the ratio of the precursor in the two precursor delivery units has been investigated. The potential of CVS for the synthesis of nanocomposites containing iron oxide and barium titanate ultrafine crystalline nanopowders with particle size bellow 10nm is demonstrated.
| Typ des Eintrags: | Artikel |
|---|---|
| Erschienen: | 2015 |
| Autor(en): | Mojić-Lanté, Bojana ; Djenadic, Ruzica ; Chakravadhanula, Venkata Sai Kiran ; Kübel, Christian ; Srdić, Vladimir V. ; Hahn, Horst ; Mullins, W. |
| Art des Eintrags: | Bibliographie |
| Titel: | Chemical Vapor Synthesis of FeOx-BaTiO3Nanocomposites |
| Sprache: | Englisch |
| Publikationsjahr: | Juni 2015 |
| Verlag: | Wiley Blackwell, USA |
| Titel der Zeitschrift, Zeitung oder Schriftenreihe: | Journal of the American Ceramic Society |
| Jahrgang/Volume einer Zeitschrift: | 98 |
| (Heft-)Nummer: | 6 |
| DOI: | 10.1111/jace.13531 |
| Kurzbeschreibung (Abstract): | Nanocomposite powders of FeOx-BaTiO3 (FO-BTO) have been prepared by chemical vapor synthesis (CVS) in a single-step process. The optimal parameters (reactor temperature, reactor length, precursor ratio) for the synthesis were investigated in an initial step for the individual systems, iron oxide (FO), and barium titanate (BTO); and in a second step optimized for the synthesis of the nanocomposites. The solid iron precursor was thermally evaporated, whereas the solid Ba- and Ti precursors were vaporized using laser flash evaporation to obtain ultrafine crystalline FO, BTO, and FO-BTO nanoparticles. The possibility to influence the mass ratios of the two phases in FO-BTO mixture by adjusting the ratio of the precursor in the two precursor delivery units has been investigated. The potential of CVS for the synthesis of nanocomposites containing iron oxide and barium titanate ultrafine crystalline nanopowders with particle size bellow 10nm is demonstrated. |
| Fachbereich(e)/-gebiet(e): | 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Gemeinschaftslabor Nanomaterialien 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft 11 Fachbereich Material- und Geowissenschaften |
| Hinterlegungsdatum: | 10 Feb 2016 09:09 |
| Letzte Änderung: | 10 Feb 2016 09:09 |
| PPN: | |
| Sponsoren: | B. M. L. acknowledges the support of the German Academic Exchange Service for a fellowship (DAADA/11/84495) and the possibility to conduct research in the Joint Research Laboratory Nanomaterials - TU Darmstadt and KIT, Germany, for a period of 6 months., Financial support from Ministry of Science of Republic of Serbia (project III45021) is also acknowledged. |
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