Salem, Nahed M. H. ; Rashad, Amal R. ; El Sayed, Laila ; Foro, Sabine ; Haase, Wolfgang ; Iskander, Magdi F. (2015)
Synthesis, characterization, molecular structure and supramolecular architectures of some copper(II) complexes derived from salicylaldehyde semicarbazone.
In: Inorganica Chimica Acta, 432
doi: 10.1016/j.ica.2015.04.019
Artikel, Bibliographie
Kurzbeschreibung (Abstract)
A series of new copper(II) complexes, [Cu(HSalsc)Cl]center dot 1/2H(2)O (1), [{Cu(HSalsc)}(2)(NO3)(2)][{Cu(HSalsc)}(2)- NO3)center dot H2O]NO3 (2), [{Cu(Salsc)}(2)]H2O (3), [Cu(HSalsc)(HIm)]Cl center dot 1/2H(2)O (4), [{Cu(HSalsc)HIm}(2)](NO3)(2) (5) and [Cu(HSalsc)(HIm)]OAc (6) derived from salicylaldehyde semicarbazone (H(2)Salsc) have been prepared and characterized by elemental analysis, infrared and UV-Vis absorption spectra as well as electrospray mass spectra (ESI-MS). The crystal and molecular structure of 1, 2, 5 and 6 have been determined by X-ray single crystal diffraction. The supramolecular architectures in 1, 2, 5 and 6 have been also discussed. (C) 2015 Elsevier B.V. All rights reserved.
| Typ des Eintrags: | Artikel |
|---|---|
| Erschienen: | 2015 |
| Autor(en): | Salem, Nahed M. H. ; Rashad, Amal R. ; El Sayed, Laila ; Foro, Sabine ; Haase, Wolfgang ; Iskander, Magdi F. |
| Art des Eintrags: | Bibliographie |
| Titel: | Synthesis, characterization, molecular structure and supramolecular architectures of some copper(II) complexes derived from salicylaldehyde semicarbazone |
| Sprache: | Englisch |
| Publikationsjahr: | 1 Juni 2015 |
| Verlag: | ELSEVIER SCIENCE SA, Switzerland |
| Titel der Zeitschrift, Zeitung oder Schriftenreihe: | Inorganica Chimica Acta |
| Jahrgang/Volume einer Zeitschrift: | 432 |
| DOI: | 10.1016/j.ica.2015.04.019 |
| Kurzbeschreibung (Abstract): | A series of new copper(II) complexes, [Cu(HSalsc)Cl]center dot 1/2H(2)O (1), [{Cu(HSalsc)}(2)(NO3)(2)][{Cu(HSalsc)}(2)- NO3)center dot H2O]NO3 (2), [{Cu(Salsc)}(2)]H2O (3), [Cu(HSalsc)(HIm)]Cl center dot 1/2H(2)O (4), [{Cu(HSalsc)HIm}(2)](NO3)(2) (5) and [Cu(HSalsc)(HIm)]OAc (6) derived from salicylaldehyde semicarbazone (H(2)Salsc) have been prepared and characterized by elemental analysis, infrared and UV-Vis absorption spectra as well as electrospray mass spectra (ESI-MS). The crystal and molecular structure of 1, 2, 5 and 6 have been determined by X-ray single crystal diffraction. The supramolecular architectures in 1, 2, 5 and 6 have been also discussed. (C) 2015 Elsevier B.V. All rights reserved. |
| Freie Schlagworte: | Salicylaldehyde semicarbazone Cu(II) complexes, Synthesis, Characterization, X-ray crystal structures, Supramolecular architectures |
| Fachbereich(e)/-gebiet(e): | 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Strukturforschung 07 Fachbereich Chemie 11 Fachbereich Material- und Geowissenschaften |
| Hinterlegungsdatum: | 19 Jan 2016 12:50 |
| Letzte Änderung: | 19 Jan 2016 16:08 |
| PPN: | |
| Sponsoren: | Thanks are due to DFG (1.8131e-2/09) for supporting this bilateral project. |
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