Suffner, J. ; Wang, D. ; Kübel, C. ; Hahn, H. (2011)
Metastable phase formation during flame spray pyrolysis of ZrO2(Y2O3)–Al2O3 nanoparticles.
In: Scripta Materialia, 64 (8)
doi: 10.1016/j.scriptamat.20https://doi.org/10.12.040
Artikel, Bibliographie
Kurzbeschreibung (Abstract)
Nanoparticles with the composition (1 − x mol.%) [ZrO2 (3 mol.% Y2O3)]–(x mol.%) Al2O3, with x ranging from 0 to 1, were prepared by liquid-feed flame spray pyrolysis. The effect of the alumina content on the morphology and phase formation was studied by means of X-ray diffraction, nitrogen adsorption and transmission electron microscopy. It is shown that alumina can be incorporated into the nanoparticles at levels above the solubility limit, leading to the formation of metastable extended solid solutions and core–shell nanoparticles.
Typ des Eintrags: | Artikel |
---|---|
Erschienen: | 2011 |
Autor(en): | Suffner, J. ; Wang, D. ; Kübel, C. ; Hahn, H. |
Art des Eintrags: | Bibliographie |
Titel: | Metastable phase formation during flame spray pyrolysis of ZrO2(Y2O3)–Al2O3 nanoparticles |
Sprache: | Englisch |
Publikationsjahr: | April 2011 |
Verlag: | Elsevier Science Publishing Company |
Titel der Zeitschrift, Zeitung oder Schriftenreihe: | Scripta Materialia |
Jahrgang/Volume einer Zeitschrift: | 64 |
(Heft-)Nummer: | 8 |
DOI: | 10.1016/j.scriptamat.20https://doi.org/10.12.040 |
Kurzbeschreibung (Abstract): | Nanoparticles with the composition (1 − x mol.%) [ZrO2 (3 mol.% Y2O3)]–(x mol.%) Al2O3, with x ranging from 0 to 1, were prepared by liquid-feed flame spray pyrolysis. The effect of the alumina content on the morphology and phase formation was studied by means of X-ray diffraction, nitrogen adsorption and transmission electron microscopy. It is shown that alumina can be incorporated into the nanoparticles at levels above the solubility limit, leading to the formation of metastable extended solid solutions and core–shell nanoparticles. |
Freie Schlagworte: | Nanocrystalline materials, X-ray diffraction (XRD), Ceramics, Phase transformation, Annealing |
Fachbereich(e)/-gebiet(e): | 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Gemeinschaftslabor Nanomaterialien 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft 11 Fachbereich Material- und Geowissenschaften |
Hinterlegungsdatum: | 19 Feb 2013 09:40 |
Letzte Änderung: | 05 Mär 2013 10:05 |
PPN: | |
Sponsoren: | The financial support by the State of Hesse (Germany) is gratefully acknowledged. |
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