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Mechanical alloying of Fe–Si and milling of α- and β-FeSi2 bulk phases

Dézsi, I. ; Fetzer, Cs. ; Bujdosó, L. ; Brötz, J. ; Balogh, A. G. (2010)
Mechanical alloying of Fe–Si and milling of α- and β-FeSi2 bulk phases.
In: Journal of Alloys and Compounds, 508 (1)
doi: 10.1016/j.jallcom.2010.07.178
Artikel, Bibliographie

Kurzbeschreibung (Abstract)

Iron disilicide synthesis by mechanical alloying was performed. ɛ-FeSi, α-Fe1−xSi2, amorphous FeSi2 were formed with relative intensities depending on the milling period. β-FeSi2 phase was formed after annealing the gridded powder at the temperature where this phase is stable. Mössbauer spectroscopy and X-ray diffraction methods were applied to determine the different phases formed. The morphology of the resulting particles was observed by high resolution scanning electron microscopy. The effect of the milling on bulk iron–silicide samples was and studied chemical effects of the ball milling on Fe–Si2 systems have been studied.

Typ des Eintrags: Artikel
Erschienen: 2010
Autor(en): Dézsi, I. ; Fetzer, Cs. ; Bujdosó, L. ; Brötz, J. ; Balogh, A. G.
Art des Eintrags: Bibliographie
Titel: Mechanical alloying of Fe–Si and milling of α- and β-FeSi2 bulk phases
Sprache: Englisch
Publikationsjahr: 15 Oktober 2010
Verlag: Elsevier Science Publishing Company
Titel der Zeitschrift, Zeitung oder Schriftenreihe: Journal of Alloys and Compounds
Jahrgang/Volume einer Zeitschrift: 508
(Heft-)Nummer: 1
DOI: 10.1016/j.jallcom.2010.07.178
Kurzbeschreibung (Abstract):

Iron disilicide synthesis by mechanical alloying was performed. ɛ-FeSi, α-Fe1−xSi2, amorphous FeSi2 were formed with relative intensities depending on the milling period. β-FeSi2 phase was formed after annealing the gridded powder at the temperature where this phase is stable. Mössbauer spectroscopy and X-ray diffraction methods were applied to determine the different phases formed. The morphology of the resulting particles was observed by high resolution scanning electron microscopy. The effect of the milling on bulk iron–silicide samples was and studied chemical effects of the ball milling on Fe–Si2 systems have been studied.

Freie Schlagworte: Mechanical alloying; Iron–silicide phases; Mössbauer; XRD
Fachbereich(e)/-gebiet(e): 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Materialanalytik
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Strukturforschung
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft
11 Fachbereich Material- und Geowissenschaften
Hinterlegungsdatum: 11 Dez 2012 10:22
Letzte Änderung: 05 Mär 2013 10:04
PPN:
Sponsoren: The financial support of the collaborative research center sSFBd Grant No. 595 of the Deutsche Forschungsgemeinschaft sDFGd is greatly appreciated.
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