Kroke, Edwin ; Loeffler, Lars ; Lange, Fred F. ; Riedel, Ralf (2002)
Aluminum Nitride Prepared by Nitridation of Aluminum Oxide Precursors.
4th International Conference on Advanced Ceramics and Glasses. MAUI, HAWAII (04.11.2001-08.11.2001)
doi: 10.1111/j.1151-2916.2002.tb00595.x
Konferenzveröffentlichung, Bibliographie
Kurzbeschreibung (Abstract)
Aluminum nitride (AlN) powders were prepared from the oxide precursors aluminum nitrate, aluminum hydroxide, aluminum 2-ethyl-hexanoate, and aluminum isopropoxide (i.e., Al(NO3)3, Al(OH)3, Al(OH)(O2CCH(C2H5)(C4H9))2, and Al(OCH(CH3)2)3). Pyrolyses were performed in flowing dry NH3 and N2 at 1000°–1500°C. For comparison, the nitride precursors aluminum dimethylamide (Al(N(CH3)2)3) and aluminum trimethylamino alane (AlH3�N(CH3)3) were exposed to the same nitridation conditions. Products were investigated using XRD, TEM, EDX, SEM, and elemental analysis. The results showed that nitridation was primarily controlled by the water:ammonia ratio in the atmosphere. Single-phase AlN powders were obtained from all oxide precursors. Complete nitridation was not obtained using pure N2, even for the non-oxide precursors.
| Typ des Eintrags: | Konferenzveröffentlichung |
|---|---|
| Erschienen: | 2002 |
| Autor(en): | Kroke, Edwin ; Loeffler, Lars ; Lange, Fred F. ; Riedel, Ralf |
| Art des Eintrags: | Bibliographie |
| Titel: | Aluminum Nitride Prepared by Nitridation of Aluminum Oxide Precursors |
| Sprache: | Englisch |
| Publikationsjahr: | Dezember 2002 |
| Verlag: | AMER CHEMICAL SOC, WASHINGTON, USA |
| Titel der Zeitschrift, Zeitung oder Schriftenreihe: | Journal of the American Ceramic Society |
| (Heft-)Nummer: | 12 |
| Reihe: | Journal of the American Ceramic Society |
| Band einer Reihe: | 85 (12) |
| Veranstaltungstitel: | 4th International Conference on Advanced Ceramics and Glasses |
| Veranstaltungsort: | MAUI, HAWAII |
| Veranstaltungsdatum: | 04.11.2001-08.11.2001 |
| DOI: | 10.1111/j.1151-2916.2002.tb00595.x |
| URL / URN: | https://onlinelibrary.wiley.com/doi/abs/10.1111/j.1151-2916.... |
| Kurzbeschreibung (Abstract): | Aluminum nitride (AlN) powders were prepared from the oxide precursors aluminum nitrate, aluminum hydroxide, aluminum 2-ethyl-hexanoate, and aluminum isopropoxide (i.e., Al(NO3)3, Al(OH)3, Al(OH)(O2CCH(C2H5)(C4H9))2, and Al(OCH(CH3)2)3). Pyrolyses were performed in flowing dry NH3 and N2 at 1000°–1500°C. For comparison, the nitride precursors aluminum dimethylamide (Al(N(CH3)2)3) and aluminum trimethylamino alane (AlH3�N(CH3)3) were exposed to the same nitridation conditions. Products were investigated using XRD, TEM, EDX, SEM, and elemental analysis. The results showed that nitridation was primarily controlled by the water:ammonia ratio in the atmosphere. Single-phase AlN powders were obtained from all oxide precursors. Complete nitridation was not obtained using pure N2, even for the non-oxide precursors. |
| Freie Schlagworte: | POWDERS; ALN; CERAMICS; ROUTES; FILMS; AIN |
| Fachbereich(e)/-gebiet(e): | 11 Fachbereich Material- und Geowissenschaften 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Disperse Feststoffe |
| Hinterlegungsdatum: | 26 Apr 2012 11:10 |
| Letzte Änderung: | 21 Aug 2018 14:46 |
| PPN: | |
| Sponsoren: | E. K. acknowledges the A.v. Humboldt Foundation for granting a Feodor Lynen Fellowship. A portion of E. K.’s salary was supported through funds from a Max Planck International Research Award., Nonsalary support came from the Materials Research Laboratory Program of the National Science Foundation under award No. DMR96–32716., The study was also supported, in part, by the Fonds der Chemischen Industrie (FCI, Frankfurt, Germany). |
| Export: | |
| Suche nach Titel in: | TUfind oder in Google |
 |
Frage zum Eintrag |
Optionen (nur für Redakteure)
 |
Redaktionelle Details anzeigen |
Drucken
Impressum