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Monoclinic Zirconia Bodies by Thermoplastic Ceramic Extrusion

Scheying, Gerd ; Wührl, Ingrid ; Eisele, Ulrich ; Riedel, Ralf (2004)
Monoclinic Zirconia Bodies by Thermoplastic Ceramic Extrusion.
In: Journal of the American Ceramic Society, 87 (3)
Artikel, Bibliographie

Kurzbeschreibung (Abstract)

wo ultrafine, undoped ZrO2 powders with median primary particle sizes of 9 and 25 nm were used to prepare ceramic suspensions for thermoplastic extrusion. The organic vehicle consisted of an industrial-grade poly(ethylene-co-vinyl acetate) (EVA) or polyethylene (PE-HD) and decanoic acid as a dispersing agent. The powder volume loadings achieved were 44% and 52% by volume for the two powders, respectively. The amount of dispersant needed was calculated from a new model based on available chemisorption sites on the powder surface. Mixing and extrusion were conducted using a conventional modular plastic processing unit. Green bodies were dewaxed up to 450°C in an inert atmosphere and sintered to full density in air at 1060° and 1100°C, respectively. Analysis of the ceramic phase content and the microstructure of the bodies is presented.

Typ des Eintrags: Artikel
Erschienen: 2004
Autor(en): Scheying, Gerd ; Wührl, Ingrid ; Eisele, Ulrich ; Riedel, Ralf
Art des Eintrags: Bibliographie
Titel: Monoclinic Zirconia Bodies by Thermoplastic Ceramic Extrusion
Sprache: Englisch
Publikationsjahr: 23 März 2004
Verlag: Wiley
Titel der Zeitschrift, Zeitung oder Schriftenreihe: Journal of the American Ceramic Society
Jahrgang/Volume einer Zeitschrift: 87
(Heft-)Nummer: 3
Kurzbeschreibung (Abstract):

wo ultrafine, undoped ZrO2 powders with median primary particle sizes of 9 and 25 nm were used to prepare ceramic suspensions for thermoplastic extrusion. The organic vehicle consisted of an industrial-grade poly(ethylene-co-vinyl acetate) (EVA) or polyethylene (PE-HD) and decanoic acid as a dispersing agent. The powder volume loadings achieved were 44% and 52% by volume for the two powders, respectively. The amount of dispersant needed was calculated from a new model based on available chemisorption sites on the powder surface. Mixing and extrusion were conducted using a conventional modular plastic processing unit. Green bodies were dewaxed up to 450°C in an inert atmosphere and sintered to full density in air at 1060° and 1100°C, respectively. Analysis of the ceramic phase content and the microstructure of the bodies is presented.

Freie Schlagworte: zirconia, extrusion
Fachbereich(e)/-gebiet(e): 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Disperse Feststoffe
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft
11 Fachbereich Material- und Geowissenschaften
Hinterlegungsdatum: 23 Apr 2012 08:28
Letzte Änderung: 05 Mär 2013 10:00
PPN:
Sponsoren: Supported by German Federal Grant (BMBf) under Grant No. 03M2744A5.
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