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High-Pressure Multianvil Synthesis and Structure Refinement of Oxygen-Bearing Cubic Zirconium(IV) Nitride

Dzivenko, D. A. ; Zerr, A. ; Bulatov, V. K. ; Miehe, G. ; Li, J. ; Thybusch, B. ; Brötz, J. ; Fuess, H. ; Brey, G. ; Riedel, R. (2007):
High-Pressure Multianvil Synthesis and Structure Refinement of Oxygen-Bearing Cubic Zirconium(IV) Nitride.
In: Advanced Materials, 19 (14), pp. 1869-1873. Wiley, ISSN 09359648,
[Article]

Abstract

Macroscopic amounts of oxygen-bearing c-Zr3N4with a cubic Th3P4-type structure are synthesized for the first time (see figure) at high pressures and temperatures. Structure refinement based on X-ray diffraction data is performed. The Raman spectrum, morphology, and microhardness of the synthesized material is measured.

Item Type: Article
Erschienen: 2007
Creators: Dzivenko, D. A. ; Zerr, A. ; Bulatov, V. K. ; Miehe, G. ; Li, J. ; Thybusch, B. ; Brötz, J. ; Fuess, H. ; Brey, G. ; Riedel, R.
Title: High-Pressure Multianvil Synthesis and Structure Refinement of Oxygen-Bearing Cubic Zirconium(IV) Nitride
Language: English
Abstract:

Macroscopic amounts of oxygen-bearing c-Zr3N4with a cubic Th3P4-type structure are synthesized for the first time (see figure) at high pressures and temperatures. Structure refinement based on X-ray diffraction data is performed. The Raman spectrum, morphology, and microhardness of the synthesized material is measured.

Journal or Publication Title: Advanced Materials
Journal volume: 19
Number: 14
Publisher: Wiley
Uncontrolled Keywords: Nanocrystalline materials, Nitrides, Transition metals, Zirconia
Divisions: 11 Department of Materials and Earth Sciences
11 Department of Materials and Earth Sciences > Material Science
11 Department of Materials and Earth Sciences > Material Science > Material Analytics
11 Department of Materials and Earth Sciences > Material Science > Dispersive Solids
11 Department of Materials and Earth Sciences > Material Science > Structure Research
Date Deposited: 19 Apr 2012 08:21
Official URL: http://dx.doi.org/10.1002/adma.200602610
Identification Number: doi:10.1002/adma.200602610
Funders: Funded by Deutsche Forschungsgemeinschaft
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