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Microstructural Analysis and Mechanical Characterization of Shape Memory Alloy Ni-Ti-Ag Synthesized by Casting Route

Salman, Khansaa Dawood ; Al-Maliki, Wisam Abed Kattea ; Alobaid, Falah ; Epple, Bernd (2022)
Microstructural Analysis and Mechanical Characterization of Shape Memory Alloy Ni-Ti-Ag Synthesized by Casting Route.
In: Applied Sciences, 2022, 12 (9)
doi: 10.26083/tuprints-00022071
Artikel, Zweitveröffentlichung, Verlagsversion

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Kurzbeschreibung (Abstract)

The purpose of the current research is to study the microstructure and mechanical properties of Ni-Ti-Ag shape memory alloys prepared by the casting route. Ag (grain size at 1 mm) was incorporated into Ni-Ti alloys at varying percentages of weight (0, 1.5, 3 and 4.5 wt.% Ag) to produce shape memory alloys using a Vacuum Arc Re-melting (VAR) furnace. Microstructural analysis was defined by FESEM microscopy and XRD examinations, while the transformation temperatures of the Ni-Ti-Ag shape memory alloy were determined by DSC examination. On the other hand, determination of mechanical properties was carried out using micro-hardness and compressive tests. The results of this work show that Ag was dispersed homogeneously into the Ni-Ti alloy. Moreover, two primary phases (austenite phase and martensite phase) emerged with few impurities. The results of the XRD examination show that the number of Ag peaks increased with the increase in weight percentage of Ag. The transformation temperature of the austenitic phase was defined as −1.6 ◦C by DSC. The mechanical characterizations increased with the increase in weight percentages of Ag (1.5, 3 and 4.5 wt.%), and significantly affected the mechanical properties of the Ni-Ti alloy. An improvement in compressive strength (42.478%) was found for the alloy with 3 wt.% Ag, while the micro-hardness results show a slight decrease in micro-hardness (8.858%) for the alloy with 4.5 wt.% Ag.

Typ des Eintrags: Artikel
Erschienen: 2022
Autor(en): Salman, Khansaa Dawood ; Al-Maliki, Wisam Abed Kattea ; Alobaid, Falah ; Epple, Bernd
Art des Eintrags: Zweitveröffentlichung
Titel: Microstructural Analysis and Mechanical Characterization of Shape Memory Alloy Ni-Ti-Ag Synthesized by Casting Route
Sprache: Englisch
Publikationsjahr: 2022
Ort: Darmstadt
Publikationsdatum der Erstveröffentlichung: 2022
Verlag: MDPI
Titel der Zeitschrift, Zeitung oder Schriftenreihe: Applied Sciences
Jahrgang/Volume einer Zeitschrift: 12
(Heft-)Nummer: 9
Kollation: 10 Seiten
DOI: 10.26083/tuprints-00022071
URL / URN: https://tuprints.ulb.tu-darmstadt.de/22071
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Herkunft: Zweitveröffentlichung aus gefördertem Golden Open Access
Kurzbeschreibung (Abstract):

The purpose of the current research is to study the microstructure and mechanical properties of Ni-Ti-Ag shape memory alloys prepared by the casting route. Ag (grain size at 1 mm) was incorporated into Ni-Ti alloys at varying percentages of weight (0, 1.5, 3 and 4.5 wt.% Ag) to produce shape memory alloys using a Vacuum Arc Re-melting (VAR) furnace. Microstructural analysis was defined by FESEM microscopy and XRD examinations, while the transformation temperatures of the Ni-Ti-Ag shape memory alloy were determined by DSC examination. On the other hand, determination of mechanical properties was carried out using micro-hardness and compressive tests. The results of this work show that Ag was dispersed homogeneously into the Ni-Ti alloy. Moreover, two primary phases (austenite phase and martensite phase) emerged with few impurities. The results of the XRD examination show that the number of Ag peaks increased with the increase in weight percentage of Ag. The transformation temperature of the austenitic phase was defined as −1.6 ◦C by DSC. The mechanical characterizations increased with the increase in weight percentages of Ag (1.5, 3 and 4.5 wt.%), and significantly affected the mechanical properties of the Ni-Ti alloy. An improvement in compressive strength (42.478%) was found for the alloy with 3 wt.% Ag, while the micro-hardness results show a slight decrease in micro-hardness (8.858%) for the alloy with 4.5 wt.% Ag.

Freie Schlagworte: shape memory alloys; Ni-Ti-Ag; casting; VAR furnace; microstructure; XRD; mechanical properties
Status: Verlagsversion
URN: urn:nbn:de:tuda-tuprints-220716
Sachgruppe der Dewey Dezimalklassifikatin (DDC): 600 Technik, Medizin, angewandte Wissenschaften > 600 Technik
600 Technik, Medizin, angewandte Wissenschaften > 620 Ingenieurwissenschaften und Maschinenbau
Fachbereich(e)/-gebiet(e): 16 Fachbereich Maschinenbau
16 Fachbereich Maschinenbau > Institut für Energiesysteme und Energietechnik (EST)
Hinterlegungsdatum: 24 Aug 2022 12:22
Letzte Änderung: 25 Aug 2022 06:20
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