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Mapping humidity-dependent mechanical properties of a single cellulose fibre

Auernhammer, Julia ; Keil, Tom ; Lin, Binbin ; Schäfer, Jan-Lukas ; Xu, Bai-Xiang ; Biesalski, Markus ; Stark, Robert W. (2021)
Mapping humidity-dependent mechanical properties of a single cellulose fibre.
In: Cellulose, 28 (13)
doi: 10.1007/s10570-021-04058-4
Artikel, Bibliographie

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Kurzbeschreibung (Abstract)

Modelling of single cellulose fibres is usually performed by assuming homogenous properties, such as strength and Young’s modulus, for the whole fibre. Additionally, the inhomogeneity in size and swelling behaviour along the fibre is often disregarded. For better numerical models, a more detailed characterisation of the fibre is required. Herein, we report a method based on atomic force microscopy to map these properties along the fibre. A fibre was mechanically characterised by static colloidal probe AFM measurements along the longitudinal direction of the fibre. Thus, the contact stress and strain at each loading point could be extracted. Stress–strain curves were be obtained along the fibre. Additionally, mechanical properties such as adhesion or dissipation were mapped. Local variations of the effective fibre radius were recorded via confocal laser scanning microscopy. Scanning electron microscopy measurements revealed the local macroscopic fibril orientation and provided an overview of the fibre topography. By combining these data, regions along the fibre with higher adhesion, dissipation, bending ability and strain or differences in the contact stress when increasing the relative humidity could be identified. This combined approach allows for one to obtain a detailed picture of the mechanical properties of single fibres.

Typ des Eintrags: Artikel
Erschienen: 2021
Autor(en): Auernhammer, Julia ; Keil, Tom ; Lin, Binbin ; Schäfer, Jan-Lukas ; Xu, Bai-Xiang ; Biesalski, Markus ; Stark, Robert W.
Art des Eintrags: Bibliographie
Titel: Mapping humidity-dependent mechanical properties of a single cellulose fibre
Sprache: Englisch
Publikationsjahr: 14 Juli 2021
Verlag: Springer Science
Titel der Zeitschrift, Zeitung oder Schriftenreihe: Cellulose
Jahrgang/Volume einer Zeitschrift: 28
(Heft-)Nummer: 13
DOI: 10.1007/s10570-021-04058-4
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Kurzbeschreibung (Abstract):

Modelling of single cellulose fibres is usually performed by assuming homogenous properties, such as strength and Young’s modulus, for the whole fibre. Additionally, the inhomogeneity in size and swelling behaviour along the fibre is often disregarded. For better numerical models, a more detailed characterisation of the fibre is required. Herein, we report a method based on atomic force microscopy to map these properties along the fibre. A fibre was mechanically characterised by static colloidal probe AFM measurements along the longitudinal direction of the fibre. Thus, the contact stress and strain at each loading point could be extracted. Stress–strain curves were be obtained along the fibre. Additionally, mechanical properties such as adhesion or dissipation were mapped. Local variations of the effective fibre radius were recorded via confocal laser scanning microscopy. Scanning electron microscopy measurements revealed the local macroscopic fibril orientation and provided an overview of the fibre topography. By combining these data, regions along the fibre with higher adhesion, dissipation, bending ability and strain or differences in the contact stress when increasing the relative humidity could be identified. This combined approach allows for one to obtain a detailed picture of the mechanical properties of single fibres.

Fachbereich(e)/-gebiet(e): 11 Fachbereich Material- und Geowissenschaften
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Mechanik Funktionaler Materialien
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Physikalische Metallkunde
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Physics of Surfaces
07 Fachbereich Chemie
07 Fachbereich Chemie > Ernst-Berl-Institut
07 Fachbereich Chemie > Ernst-Berl-Institut > Fachgebiet Makromolekulare Chemie
Zentrale Einrichtungen
Zentrale Einrichtungen > Hochschulrechenzentrum (HRZ)
Zentrale Einrichtungen > Hochschulrechenzentrum (HRZ) > Hochleistungsrechner
Hinterlegungsdatum: 21 Jul 2021 09:04
Letzte Änderung: 11 Dez 2024 07:55
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