Schultheiß, Jan ; Porz, Lukas ; Kodumudi Venkataraman, Lalitha ; Höfling, Marion ; Yildirim, Can ; Cook, Phil ; Detlefs, Carsten ; Gorfman, Semen ; Rödel, Jürgen ; Simons, Hugh (2021)
Quantitative mapping of nanotwin variants in the bulk.
In: Scripta Materialia, 199
doi: 10.1016/j.scriptamat.2021.113878
Artikel, Bibliographie
Dies ist die neueste Version dieses Eintrags.
Kurzbeschreibung (Abstract)
Crystallographic twins are critical to the properties of numerous materials from magnesium alloys to piezoelectrics. Since the onset of the twin formation is highly sensitive to the triaxial mechanical bound- ary conditions, non-destructive bulk microscopy techniques are required. Elastic strains can be mapped via X-ray diffraction with a 10 0-20 0 nm resolution. However, the interplay of strains with nanotwins cannot be characterized. Here, a method based on dark-field X-ray microscopy to quantify the density of nanotwin variants with twin lamellae of sizes as small as several tens of nanometers in embedded sub- volumes (70x20 0x60 0 nm 3 ) in millimeter-sized samples is introduced. The methodology is corroborated by correlating the local density of twin variants to the long-ranging strain fields for a high-performance piezoelectric material. The method facilitates direct, in situ mapping and quantification of nanoscale struc- tural changes together with their elastic driving fields, which is the key towards controlling and engineer- ing material’s performance at nanometric scales.
| Typ des Eintrags: | Artikel |
|---|---|
| Erschienen: | 2021 |
| Autor(en): | Schultheiß, Jan ; Porz, Lukas ; Kodumudi Venkataraman, Lalitha ; Höfling, Marion ; Yildirim, Can ; Cook, Phil ; Detlefs, Carsten ; Gorfman, Semen ; Rödel, Jürgen ; Simons, Hugh |
| Art des Eintrags: | Bibliographie |
| Titel: | Quantitative mapping of nanotwin variants in the bulk |
| Sprache: | Englisch |
| Publikationsjahr: | 29 März 2021 |
| Verlag: | Elsevier Science Publishing |
| Titel der Zeitschrift, Zeitung oder Schriftenreihe: | Scripta Materialia |
| Jahrgang/Volume einer Zeitschrift: | 199 |
| DOI: | 10.1016/j.scriptamat.2021.113878 |
| URL / URN: | https://www.sciencedirect.com/science/article/pii/S135964622... |
| Zugehörige Links: | |
| Kurzbeschreibung (Abstract): | Crystallographic twins are critical to the properties of numerous materials from magnesium alloys to piezoelectrics. Since the onset of the twin formation is highly sensitive to the triaxial mechanical bound- ary conditions, non-destructive bulk microscopy techniques are required. Elastic strains can be mapped via X-ray diffraction with a 10 0-20 0 nm resolution. However, the interplay of strains with nanotwins cannot be characterized. Here, a method based on dark-field X-ray microscopy to quantify the density of nanotwin variants with twin lamellae of sizes as small as several tens of nanometers in embedded sub- volumes (70x20 0x60 0 nm 3 ) in millimeter-sized samples is introduced. The methodology is corroborated by correlating the local density of twin variants to the long-ranging strain fields for a high-performance piezoelectric material. The method facilitates direct, in situ mapping and quantification of nanoscale struc- tural changes together with their elastic driving fields, which is the key towards controlling and engineer- ing material’s performance at nanometric scales. |
| Freie Schlagworte: | Twinning X-ray diffraction, Domains, Ferroelectricity, Elasto-morphological coupling |
| Fachbereich(e)/-gebiet(e): | 11 Fachbereich Material- und Geowissenschaften 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Nichtmetallisch-Anorganische Werkstoffe |
| Hinterlegungsdatum: | 31 Mär 2021 05:59 |
| Letzte Änderung: | 03 Jul 2024 02:51 |
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| Suche nach Titel in: | TUfind oder in Google |
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Quantitative mapping of nanotwin variants in the bulk. (deposited 10 Feb 2023 09:24)
- Quantitative mapping of nanotwin variants in the bulk. (deposited 31 Mär 2021 05:59) [Gegenwärtig angezeigt]
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