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Atomically stable cryogenic in situ biasing (S)TEM holder with precise temperature control over a wide range of temperatures

Andersen, Mia ; Pivak, Yevheniy ; Papadimitriou, Vasilis ; Jiang, Tianshu ; Roddatis, Vladimir ; Molina-Luna, Leopoldo ; Conroy, Michele (2024)
Atomically stable cryogenic in situ biasing (S)TEM holder with precise temperature control over a wide range of temperatures.
In: Microscopy and Microanalysis, 30 (Suppl. 1)
doi: 10.1093/mam/ozae044.687
Article, Bibliographie

Abstract

Cryo scanning transmission electron microscopy (STEM) is becoming an indispensable tool for studying phase transitions in various quantum materials [1-3] at the atomic scale. A detailed characterization of a sample’s structural and electronic properties across phase transitions necessitates a sample holder with double tilt capability and a continuous temperature control of the specimen while maintaining a sample stability that enables atomic resolution imaging. Temperature control is achieved using microelectromechanical systems (MEMS)-based heating and biasing chips [4, 5] in combination with a dedicated cryo TEM sample holder.

Item Type: Article
Erschienen: 2024
Creators: Andersen, Mia ; Pivak, Yevheniy ; Papadimitriou, Vasilis ; Jiang, Tianshu ; Roddatis, Vladimir ; Molina-Luna, Leopoldo ; Conroy, Michele
Type of entry: Bibliographie
Title: Atomically stable cryogenic in situ biasing (S)TEM holder with precise temperature control over a wide range of temperatures
Language: English
Date: 24 July 2024
Publisher: Oxford University Press
Journal or Publication Title: Microscopy and Microanalysis
Volume of the journal: 30
Issue Number: Suppl. 1
DOI: 10.1093/mam/ozae044.687
Abstract:

Cryo scanning transmission electron microscopy (STEM) is becoming an indispensable tool for studying phase transitions in various quantum materials [1-3] at the atomic scale. A detailed characterization of a sample’s structural and electronic properties across phase transitions necessitates a sample holder with double tilt capability and a continuous temperature control of the specimen while maintaining a sample stability that enables atomic resolution imaging. Temperature control is achieved using microelectromechanical systems (MEMS)-based heating and biasing chips [4, 5] in combination with a dedicated cryo TEM sample holder.

Additional Information:

Physical Sciences Symposia: Advanced Imaging and Spectroscopy Beyond Room Temperature

Divisions: 11 Department of Materials and Earth Sciences
11 Department of Materials and Earth Sciences > Material Science
11 Department of Materials and Earth Sciences > Material Science > Advanced Electron Microscopy (aem)
Date Deposited: 31 Jul 2024 06:46
Last Modified: 31 Jul 2024 06:46
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