Doran, A. ; Schlicker, Lukas ; Beavers, C. M. ; Bhat, Shrikant ; Bekheet, Maged F. ; Gurlo, Aleksander (2017):
Compact low power infrared tube furnace for in situ X-ray powder diffraction.
In: Review of Scientific Instruments, 88 (1), pp. 013903. American Institute of Physics, Melville, USA, ISSN 0034-6748,
DOI: 10.1063/1.4973561,
[Article]
Abstract
We describe the development and implementation of a compact, low power, infrared heated tube furnace for in situ powder X-ray diffraction experiments. Our silicon carbide (SiC) based furnace design exhibits outstanding thermal performance in terms of accuracy control and temperature ramping rates while simultaneously being easy to use, robust to abuse and, due to its small size and low power, producing minimal impact on surrounding equipment. Temperatures in air in excess of 1100 degrees C can be controlled at an accuracy of better than 1%, with temperature ramping rates up to 100 degrees C/s. The complete "add-in" device, minus power supply, fits in a cylindrical volume approximately 15 cm long and 6 cm in diameter and resides as close as 1 cm from other sensitive components of our experimental synchrotron endstation without adverse effects.
| Item Type: | Article |
|---|---|
| Erschienen: | 2017 |
| Creators: | Doran, A. ; Schlicker, Lukas ; Beavers, C. M. ; Bhat, Shrikant ; Bekheet, Maged F. ; Gurlo, Aleksander |
| Title: | Compact low power infrared tube furnace for in situ X-ray powder diffraction |
| Language: | English |
| Abstract: | We describe the development and implementation of a compact, low power, infrared heated tube furnace for in situ powder X-ray diffraction experiments. Our silicon carbide (SiC) based furnace design exhibits outstanding thermal performance in terms of accuracy control and temperature ramping rates while simultaneously being easy to use, robust to abuse and, due to its small size and low power, producing minimal impact on surrounding equipment. Temperatures in air in excess of 1100 degrees C can be controlled at an accuracy of better than 1%, with temperature ramping rates up to 100 degrees C/s. The complete "add-in" device, minus power supply, fits in a cylindrical volume approximately 15 cm long and 6 cm in diameter and resides as close as 1 cm from other sensitive components of our experimental synchrotron endstation without adverse effects. |
| Journal or Publication Title: | Review of Scientific Instruments |
| Volume of the journal: | 88 |
| Issue Number: | 1 |
| Publisher: | American Institute of Physics, Melville, USA |
| Uncontrolled Keywords: | Thermal-Expansion, Corundum, IN2O3 |
| Divisions: | 11 Department of Materials and Earth Sciences 11 Department of Materials and Earth Sciences > Material Science 11 Department of Materials and Earth Sciences > Material Science > Dispersive Solids |
| Date Deposited: | 22 Aug 2018 14:17 |
| DOI: | 10.1063/1.4973561 |
| URL / URN: | https://aip.scitation.org/doi/10.1063/1.4973561 |
| PPN: | |
| Funders: | Office of Science, Office of Basic Energy Sciences, of the U.S. Department of Energy: DE-AC02-05CH11231, COMPRES, tConsortium for Materials Properties Research in Earth Sciences under NSF: EAR 11-57758, German Research Foundation (DFG): SPP 1415, GU 992/12-1, Advanced Light Source BL12.2.2 for beam time: DD00087 |
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