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Metastable phase formation during flame spray pyrolysis of ZrO2(Y2O3)–Al2O3 nanoparticles

Suffner, J. ; Wang, D. ; Kübel, C. ; Hahn, H. (2011)
Metastable phase formation during flame spray pyrolysis of ZrO2(Y2O3)–Al2O3 nanoparticles.
In: Scripta Materialia, 64 (8)
doi: 10.1016/j.scriptamat.20https://doi.org/10.12.040
Artikel, Bibliographie

Kurzbeschreibung (Abstract)

Nanoparticles with the composition (1 − x mol.%) [ZrO2 (3 mol.% Y2O3)]–(x mol.%) Al2O3, with x ranging from 0 to 1, were prepared by liquid-feed flame spray pyrolysis. The effect of the alumina content on the morphology and phase formation was studied by means of X-ray diffraction, nitrogen adsorption and transmission electron microscopy. It is shown that alumina can be incorporated into the nanoparticles at levels above the solubility limit, leading to the formation of metastable extended solid solutions and core–shell nanoparticles.

Typ des Eintrags: Artikel
Erschienen: 2011
Autor(en): Suffner, J. ; Wang, D. ; Kübel, C. ; Hahn, H.
Art des Eintrags: Bibliographie
Titel: Metastable phase formation during flame spray pyrolysis of ZrO2(Y2O3)–Al2O3 nanoparticles
Sprache: Englisch
Publikationsjahr: April 2011
Verlag: Elsevier Science Publishing Company
Titel der Zeitschrift, Zeitung oder Schriftenreihe: Scripta Materialia
Jahrgang/Volume einer Zeitschrift: 64
(Heft-)Nummer: 8
DOI: 10.1016/j.scriptamat.20https://doi.org/10.12.040
Kurzbeschreibung (Abstract):

Nanoparticles with the composition (1 − x mol.%) [ZrO2 (3 mol.% Y2O3)]–(x mol.%) Al2O3, with x ranging from 0 to 1, were prepared by liquid-feed flame spray pyrolysis. The effect of the alumina content on the morphology and phase formation was studied by means of X-ray diffraction, nitrogen adsorption and transmission electron microscopy. It is shown that alumina can be incorporated into the nanoparticles at levels above the solubility limit, leading to the formation of metastable extended solid solutions and core–shell nanoparticles.

Freie Schlagworte: Nanocrystalline materials, X-ray diffraction (XRD), Ceramics, Phase transformation, Annealing
Fachbereich(e)/-gebiet(e): 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Gemeinschaftslabor Nanomaterialien
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft
11 Fachbereich Material- und Geowissenschaften
Hinterlegungsdatum: 19 Feb 2013 09:40
Letzte Änderung: 05 Mär 2013 10:05
PPN:
Sponsoren: The financial support by the State of Hesse (Germany) is gratefully acknowledged.
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