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A Swagelok-type in situ cell for battery investigations using synchrotron radiation

Nikolowski, Kristian and Baehtz, Carsten and Bramnik, Natalia N. and Ehrenberg, Helmut (2005):
A Swagelok-type in situ cell for battery investigations using synchrotron radiation.
In: Journal of Applied Crystallography, pp. 851-853, 38, (5), ISSN 0021-8898, [Online-Edition: http://dx.doi.org/10.1107/S0021889805022302],
[Article]

Abstract

An in situ cell designed for synchrotron X-ray diffraction during electrochemical cycling of battery materials is presented. The cell operates in transmission mode and can be oscillated with the dedicated sample holder to improve powder statistics. It allows fast data acquisition, provides hermetic sealing and high-quality diffraction data, and is easy to assemble, since a commercially available Swagelok junction is used as the cell body. Diffraction data from the cycling of a battery using LixNi0.8Co0.2O2 (0 [less-than or equal to] x [less-than or equal to] 1) as the cathode material are presented.

Item Type: Article
Erschienen: 2005
Creators: Nikolowski, Kristian and Baehtz, Carsten and Bramnik, Natalia N. and Ehrenberg, Helmut
Title: A Swagelok-type in situ cell for battery investigations using synchrotron radiation
Language: English
Abstract:

An in situ cell designed for synchrotron X-ray diffraction during electrochemical cycling of battery materials is presented. The cell operates in transmission mode and can be oscillated with the dedicated sample holder to improve powder statistics. It allows fast data acquisition, provides hermetic sealing and high-quality diffraction data, and is easy to assemble, since a commercially available Swagelok junction is used as the cell body. Diffraction data from the cycling of a battery using LixNi0.8Co0.2O2 (0 [less-than or equal to] x [less-than or equal to] 1) as the cathode material are presented.

Journal or Publication Title: Journal of Applied Crystallography
Volume: 38
Number: 5
Uncontrolled Keywords: battery cell; Swagelok junction.
Divisions: 11 Department of Materials and Earth Sciences
DFG-Collaborative Research Centres (incl. Transregio)
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres
Zentrale Einrichtungen
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue > B - Characterisation
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue > B - Characterisation > Subproject B4: In situ investigations of the degradation of intercalation batteries and their modelling
Date Deposited: 15 Aug 2011 10:48
Official URL: http://dx.doi.org/10.1107/S0021889805022302
Additional Information:

SFB 595 B4

Identification Number: doi:10.1107/S0021889805022302
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