Gonzalo, E. C. and Morán, E. and Parada, C. and Ehrenberg, Helmut (2010):
Microwave-assisted synthesis of LiCoO2 and LiCo1−xGaxO2: Structural features, magnetism and electrochemical characterization.
121, In: Materials Chemistry and Physics, (3), pp. 484-488, ISSN 02540584, [Online-Edition: http://dx.doi.org/10.1016/j.matchemphys.2010.02.011],
[Article]
Abstract
Nanocrystalline (between 30 and 40 nm) LiCoO2 and LiCo1−xGaxO2 (0 ≤ x ≤ 0.15) powders have been prepared by using a standard microwave furnace.
Depending on the power and irradiation time, nanosized LT-LiCo1−xGaxO2 (cubic) or HT-LiCo1−xGaxO2 (hexagonal) (0 ≤ x ≤ 0.15) materials have been obtained and studied by means of X-ray diffraction, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Electrochemical characterization and magnetic behaviour of the electrochemical active polymorphs (HT-phases) have also been investigated.
| Item Type: | Article |
|---|---|
| Erschienen: | 2010 |
| Creators: | Gonzalo, E. C. and Morán, E. and Parada, C. and Ehrenberg, Helmut |
| Title: | Microwave-assisted synthesis of LiCoO2 and LiCo1−xGaxO2: Structural features, magnetism and electrochemical characterization |
| Language: | English |
| Abstract: | Nanocrystalline (between 30 and 40 nm) LiCoO2 and LiCo1−xGaxO2 (0 ≤ x ≤ 0.15) powders have been prepared by using a standard microwave furnace. Depending on the power and irradiation time, nanosized LT-LiCo1−xGaxO2 (cubic) or HT-LiCo1−xGaxO2 (hexagonal) (0 ≤ x ≤ 0.15) materials have been obtained and studied by means of X-ray diffraction, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Electrochemical characterization and magnetic behaviour of the electrochemical active polymorphs (HT-phases) have also been investigated. |
| Journal or Publication Title: | Materials Chemistry and Physics |
| Volume: | 121 |
| Number: | 3 |
| Uncontrolled Keywords: | Microwave synthesis; Nanosized materials; Lithium cobalt oxide; Lithium-ion batteries |
| Divisions: | DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue > B - Characterisation > Subproject B4: In situ investigations of the degradation of intercalation batteries and their modelling DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue > B - Characterisation DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue Zentrale Einrichtungen DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres DFG-Collaborative Research Centres (incl. Transregio) |
| Date Deposited: | 15 Aug 2011 09:08 |
| Official URL: | http://dx.doi.org/10.1016/j.matchemphys.2010.02.011 |
| Additional Information: | SFB 595 B4 |
| Identification Number: | doi:10.1016/j.matchemphys.2010.02.011 |
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