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In situ hot-stage transmission electron microscopy of Pb(Zr0.52Ti0.48)O3

Schmitt, Ljubomira A. and Theissmann, Ralf and Kling, Jens and Kungl, Hans and Hoffmann, Michael J. and Fuess, Hartmut (2008):
In situ hot-stage transmission electron microscopy of Pb(Zr0.52Ti0.48)O3.
In: Phase Transitions, pp. 323-329, 81, (4), ISSN 0141-1594, [Online-Edition: http://dx.doi.org/10.1080/01411590701695778],
[Article]

Abstract

The domain structure of Pb(Zr0.52Ti0.48)O3 before and after hot-stage experiment has been studied. The influence of maximum temperature, heating and cooling rate on the domain configuration of Pb(Zr1− x , Ti x )O3 with x = 0.40, 0.45, 0.48 and 0.55 was analysed. A reliable basis for further hot-stage experiments of Pb(Zr1−x, Tix)O3 has been established. The investigations revealed a temperature dependent appearance and disappearance of nano- and microdomains. The appearance of microdomains in the nano scale range during cooling, denoted as domain miniaturisation, and the time dependent recovering of the former domain structure, revealed that under specific experimental conditions the domain configuration is reversible.

Item Type: Article
Erschienen: 2008
Creators: Schmitt, Ljubomira A. and Theissmann, Ralf and Kling, Jens and Kungl, Hans and Hoffmann, Michael J. and Fuess, Hartmut
Title: In situ hot-stage transmission electron microscopy of Pb(Zr0.52Ti0.48)O3
Language: English
Abstract:

The domain structure of Pb(Zr0.52Ti0.48)O3 before and after hot-stage experiment has been studied. The influence of maximum temperature, heating and cooling rate on the domain configuration of Pb(Zr1− x , Ti x )O3 with x = 0.40, 0.45, 0.48 and 0.55 was analysed. A reliable basis for further hot-stage experiments of Pb(Zr1−x, Tix)O3 has been established. The investigations revealed a temperature dependent appearance and disappearance of nano- and microdomains. The appearance of microdomains in the nano scale range during cooling, denoted as domain miniaturisation, and the time dependent recovering of the former domain structure, revealed that under specific experimental conditions the domain configuration is reversible.

Journal or Publication Title: Phase Transitions
Volume: 81
Number: 4
Uncontrolled Keywords: Lead zirconate titanate; In situ TEM; Nanodomain; Microdomain; Domain structure; Domain miniaturisation
Divisions: DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue > A - Synthesis > Subproject A2: Manufacturing and characterization of PZT-ceramics with defined defect chemistry
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue > B - Characterisation > Subproject B3: Structure Characterization of Piezoelectric Ceramics With Respect to Electrical Fatigue
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue > A - Synthesis
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue > B - Characterisation
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres > CRC 595: Electrical fatigue
Zentrale Einrichtungen
DFG-Collaborative Research Centres (incl. Transregio) > Collaborative Research Centres
DFG-Collaborative Research Centres (incl. Transregio)
Date Deposited: 27 Jul 2011 11:27
Official URL: http://dx.doi.org/10.1080/01411590701695778
Additional Information:

SFB 595 Cooperation A2, B3

Identification Number: doi:10.1080/01411590701695778
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