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Uniaxial viscosity of low-temperature cofired ceramic (LTCC) powder compacts determined by loading dilatometry

Xie, Rong-Jun ; Zuo, Ruzhong ; Aulbach, Emil ; Mackens, Uwe ; Hirosaki, Naoto ; Rödel, Jürgen (2005)
Uniaxial viscosity of low-temperature cofired ceramic (LTCC) powder compacts determined by loading dilatometry.
In: Journal of the European Ceramic Society, 25 (4)
doi: 10.1016/j.jeurceramsoc.2004.01.022
Artikel, Bibliographie

Kurzbeschreibung (Abstract)

This paper reports on the experimental determination of the uniaxial viscosity of two commercially available low-temperature cofired ceramic (LTCC) powder compacts, Ceramtape GC (glass-ceramic) and Ferro A6M (glass), by loading dilatometry. Isothermal sintering of cylindrical green compacts was carried out at temperatures ranging from 720 to 840 °C and under varying uniaxial compressive loads of 0–50 N (corresponding to 0–0.5 MPa). Both instantaneous radial and axial strains were measured during sintering. These data were analyzed by using constitutive laws for a porous sintering body and the uniaxial viscosity was calculated as a function of relative density. The activation energy for viscosity was independent of relative density and showed an average value of 668±76 kJ/mol for the Ceramtape material but was not accessible for the Ferro material. The viscosity data were compared with several theoretical models.

Typ des Eintrags: Artikel
Erschienen: 2005
Autor(en): Xie, Rong-Jun ; Zuo, Ruzhong ; Aulbach, Emil ; Mackens, Uwe ; Hirosaki, Naoto ; Rödel, Jürgen
Art des Eintrags: Bibliographie
Titel: Uniaxial viscosity of low-temperature cofired ceramic (LTCC) powder compacts determined by loading dilatometry
Sprache: Englisch
Publikationsjahr: April 2005
Titel der Zeitschrift, Zeitung oder Schriftenreihe: Journal of the European Ceramic Society
Jahrgang/Volume einer Zeitschrift: 25
(Heft-)Nummer: 4
DOI: 10.1016/j.jeurceramsoc.2004.01.022
Kurzbeschreibung (Abstract):

This paper reports on the experimental determination of the uniaxial viscosity of two commercially available low-temperature cofired ceramic (LTCC) powder compacts, Ceramtape GC (glass-ceramic) and Ferro A6M (glass), by loading dilatometry. Isothermal sintering of cylindrical green compacts was carried out at temperatures ranging from 720 to 840 °C and under varying uniaxial compressive loads of 0–50 N (corresponding to 0–0.5 MPa). Both instantaneous radial and axial strains were measured during sintering. These data were analyzed by using constitutive laws for a porous sintering body and the uniaxial viscosity was calculated as a function of relative density. The activation energy for viscosity was independent of relative density and showed an average value of 668±76 kJ/mol for the Ceramtape material but was not accessible for the Ferro material. The viscosity data were compared with several theoretical models.

Freie Schlagworte: Dilatometry; Sintering; Porosity; Glass; Glass ceramics; LTCC
Fachbereich(e)/-gebiet(e): 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Nichtmetallisch-Anorganische Werkstoffe
11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft
11 Fachbereich Material- und Geowissenschaften
Hinterlegungsdatum: 18 Mai 2011 15:19
Letzte Änderung: 05 Mär 2013 09:47
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