Luan, Xingang ; Dong, Xichao ; Li, Min ; Cheng, Laifei ; Riedel, Ralf (2022)
Properties of TiB2–PSO modified SiHfBCN-based adhesive through polymer-derived-ceramic route.
In: Ceramics International, 48 (21)
doi: 10.1016/j.ceramint.2022.07.084
Artikel, Bibliographie
Kurzbeschreibung (Abstract)
High temperature SiHfBCN-based ceramic adhesives are fabricated by polymer derived ceramic route with SiHfBCN precursors, TiB2 and polysiloxane (PSO). The phase composition and microstructure were investigated by X-ray diffraction and scanning electron microscopy, respectively and the evolution of pores was analyzed by Micron X-ray 3D Imaging System and VG Studio MAX 3.0.2 software. After heat-treating at 80 degrees C and curing at 170 degrees C in air, the adhesion strength detected in air of SiHfBCN adhesives is 3.22 MPa at room temperature (RT) and can rise to 5.47 MPa at 1000 degrees C after pyrolysis at 1000 degrees C in air for 2 h with a universal testing machine. By modifying SiHfBCN with TiB2-PSO, the adhesion strength can be enhanced to 9.49 MPa at RT and 6.37 MPa at 1000 degrees C. The results indicate that the formation of SiO2-B2O3-TiO2 ternary glasses play an important role in improving the adhesion strength. The present study broaden the high temperature adhesive family suitable for large-scale complex ceramic components in harsh environments.
| Typ des Eintrags: | Artikel |
|---|---|
| Erschienen: | 2022 |
| Autor(en): | Luan, Xingang ; Dong, Xichao ; Li, Min ; Cheng, Laifei ; Riedel, Ralf |
| Art des Eintrags: | Bibliographie |
| Titel: | Properties of TiB2–PSO modified SiHfBCN-based adhesive through polymer-derived-ceramic route |
| Sprache: | Englisch |
| Publikationsjahr: | 1 November 2022 |
| Verlag: | Elsevier |
| Titel der Zeitschrift, Zeitung oder Schriftenreihe: | Ceramics International |
| Jahrgang/Volume einer Zeitschrift: | 48 |
| (Heft-)Nummer: | 21 |
| DOI: | 10.1016/j.ceramint.2022.07.084 |
| Kurzbeschreibung (Abstract): | High temperature SiHfBCN-based ceramic adhesives are fabricated by polymer derived ceramic route with SiHfBCN precursors, TiB2 and polysiloxane (PSO). The phase composition and microstructure were investigated by X-ray diffraction and scanning electron microscopy, respectively and the evolution of pores was analyzed by Micron X-ray 3D Imaging System and VG Studio MAX 3.0.2 software. After heat-treating at 80 degrees C and curing at 170 degrees C in air, the adhesion strength detected in air of SiHfBCN adhesives is 3.22 MPa at room temperature (RT) and can rise to 5.47 MPa at 1000 degrees C after pyrolysis at 1000 degrees C in air for 2 h with a universal testing machine. By modifying SiHfBCN with TiB2-PSO, the adhesion strength can be enhanced to 9.49 MPa at RT and 6.37 MPa at 1000 degrees C. The results indicate that the formation of SiO2-B2O3-TiO2 ternary glasses play an important role in improving the adhesion strength. The present study broaden the high temperature adhesive family suitable for large-scale complex ceramic components in harsh environments. |
| Freie Schlagworte: | High temperature adhesives, TiB2, PSO, SiHfBCN, High-Temperature Adhesive, Mechanical-Properties, Preceramic Polymer, Performance, Composites, Oxidation, Strength |
| Fachbereich(e)/-gebiet(e): | 11 Fachbereich Material- und Geowissenschaften 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Disperse Feststoffe |
| Hinterlegungsdatum: | 28 Okt 2022 06:01 |
| Letzte Änderung: | 28 Okt 2022 06:01 |
| PPN: | |
| Export: | |
| Suche nach Titel in: | TUfind oder in Google |
 |
Frage zum Eintrag |
Optionen (nur für Redakteure)
 |
Redaktionelle Details anzeigen |
Drucken
Impressum