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Optimizing the Hydrothermal Carbonization of Sewage Sludge—Response Surface Methodology and the Effect of Volatile Solids

Blach, Tobias ; Engelhart, Markus (2021)
Optimizing the Hydrothermal Carbonization of Sewage Sludge—Response Surface Methodology and the Effect of Volatile Solids.
In: Water, 2021, 13 (9)
doi: 10.26083/tuprints-00019365
Artikel, Zweitveröffentlichung, Verlagsversion

Kurzbeschreibung (Abstract)

This study focuses on identifying the optimum conditions of sewage sludge hydrothermal carbonization by Box–Behnken Design and on the effects of volatile solids on heating value and on process water load. To get insight into the solid and process water characteristics, we applied the Box–Behnken Design on the hydrothermal reaction temperature (190, 220, 250 °C), reaction time (0.5, 2.25, 4 h) and pH (3.9, 5, 6.1). The response surface of the liquid phase revealed decreasing dissolved organic carbon (DOC) concentrations with increasing temperature from 9446 mg/L (190 °C) to 7402 mg/L (250 °C) at 4 h reaction time. For the same hydrothermal conditions, NH₄-N concentration increased from 754 to 1230 mg/L. Reaction temperature was identified as the most important process parameter, whereas reaction time and pH had only minor effects. Moreover, linear coefficients of the models were more decisive than the interrelation and quadratic coefficients. Volatile solids (VS) of the feedstock were found to significantly influence both the load of the process water and the change in heating value of the hydrochars. Process water load increased steadily with higher VS. The heating value only increased with more than around 65–80% VS in feedstock.

Typ des Eintrags: Artikel
Erschienen: 2021
Autor(en): Blach, Tobias ; Engelhart, Markus
Art des Eintrags: Zweitveröffentlichung
Titel: Optimizing the Hydrothermal Carbonization of Sewage Sludge—Response Surface Methodology and the Effect of Volatile Solids
Sprache: Englisch
Publikationsjahr: 2021
Publikationsdatum der Erstveröffentlichung: 2021
Verlag: MDPI
Titel der Zeitschrift, Zeitung oder Schriftenreihe: Water
Jahrgang/Volume einer Zeitschrift: 13
(Heft-)Nummer: 9
Kollation: 19 Seiten
DOI: 10.26083/tuprints-00019365
URL / URN: https://tuprints.ulb.tu-darmstadt.de/19365
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Herkunft: Zweitveröffentlichung aus gefördertem Golden Open Access
Kurzbeschreibung (Abstract):

This study focuses on identifying the optimum conditions of sewage sludge hydrothermal carbonization by Box–Behnken Design and on the effects of volatile solids on heating value and on process water load. To get insight into the solid and process water characteristics, we applied the Box–Behnken Design on the hydrothermal reaction temperature (190, 220, 250 °C), reaction time (0.5, 2.25, 4 h) and pH (3.9, 5, 6.1). The response surface of the liquid phase revealed decreasing dissolved organic carbon (DOC) concentrations with increasing temperature from 9446 mg/L (190 °C) to 7402 mg/L (250 °C) at 4 h reaction time. For the same hydrothermal conditions, NH₄-N concentration increased from 754 to 1230 mg/L. Reaction temperature was identified as the most important process parameter, whereas reaction time and pH had only minor effects. Moreover, linear coefficients of the models were more decisive than the interrelation and quadratic coefficients. Volatile solids (VS) of the feedstock were found to significantly influence both the load of the process water and the change in heating value of the hydrochars. Process water load increased steadily with higher VS. The heating value only increased with more than around 65–80% VS in feedstock.

Status: Verlagsversion
URN: urn:nbn:de:tuda-tuprints-193658
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Keywords: Box–Behnken Design; hydrothermal carbonization; process water; sewage sludge

Sachgruppe der Dewey Dezimalklassifikatin (DDC): 600 Technik, Medizin, angewandte Wissenschaften > 600 Technik
Fachbereich(e)/-gebiet(e): 13 Fachbereich Bau- und Umweltingenieurwissenschaften
13 Fachbereich Bau- und Umweltingenieurwissenschaften > Institut IWAR - Wasser- und Abfalltechnik, Umwelt- und Raumplanung
13 Fachbereich Bau- und Umweltingenieurwissenschaften > Institut IWAR - Wasser- und Abfalltechnik, Umwelt- und Raumplanung > Fachgebiet Abwassertechnik
Hinterlegungsdatum: 25 Aug 2021 12:35
Letzte Änderung: 31 Aug 2021 05:18
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