Doran, A. ; Schlicker, Lukas ; Beavers, C. M. ; Bhat, Shrikant ; Bekheet, Maged F. ; Gurlo, Aleksander (2017)
Compact low power infrared tube furnace for in situ X-ray powder diffraction.
In: Review of Scientific Instruments, 88 (1)
doi: 10.1063/1.4973561
Artikel, Bibliographie
Kurzbeschreibung (Abstract)
We describe the development and implementation of a compact, low power, infrared heated tube furnace for in situ powder X-ray diffraction experiments. Our silicon carbide (SiC) based furnace design exhibits outstanding thermal performance in terms of accuracy control and temperature ramping rates while simultaneously being easy to use, robust to abuse and, due to its small size and low power, producing minimal impact on surrounding equipment. Temperatures in air in excess of 1100 degrees C can be controlled at an accuracy of better than 1%, with temperature ramping rates up to 100 degrees C/s. The complete "add-in" device, minus power supply, fits in a cylindrical volume approximately 15 cm long and 6 cm in diameter and resides as close as 1 cm from other sensitive components of our experimental synchrotron endstation without adverse effects.
| Typ des Eintrags: | Artikel |
|---|---|
| Erschienen: | 2017 |
| Autor(en): | Doran, A. ; Schlicker, Lukas ; Beavers, C. M. ; Bhat, Shrikant ; Bekheet, Maged F. ; Gurlo, Aleksander |
| Art des Eintrags: | Bibliographie |
| Titel: | Compact low power infrared tube furnace for in situ X-ray powder diffraction |
| Sprache: | Englisch |
| Publikationsjahr: | Januar 2017 |
| Verlag: | American Institute of Physics, Melville, USA |
| Titel der Zeitschrift, Zeitung oder Schriftenreihe: | Review of Scientific Instruments |
| Jahrgang/Volume einer Zeitschrift: | 88 |
| (Heft-)Nummer: | 1 |
| DOI: | 10.1063/1.4973561 |
| URL / URN: | https://aip.scitation.org/doi/10.1063/1.4973561 |
| Kurzbeschreibung (Abstract): | We describe the development and implementation of a compact, low power, infrared heated tube furnace for in situ powder X-ray diffraction experiments. Our silicon carbide (SiC) based furnace design exhibits outstanding thermal performance in terms of accuracy control and temperature ramping rates while simultaneously being easy to use, robust to abuse and, due to its small size and low power, producing minimal impact on surrounding equipment. Temperatures in air in excess of 1100 degrees C can be controlled at an accuracy of better than 1%, with temperature ramping rates up to 100 degrees C/s. The complete "add-in" device, minus power supply, fits in a cylindrical volume approximately 15 cm long and 6 cm in diameter and resides as close as 1 cm from other sensitive components of our experimental synchrotron endstation without adverse effects. |
| Freie Schlagworte: | Thermal-Expansion, Corundum, IN2O3 |
| Fachbereich(e)/-gebiet(e): | 11 Fachbereich Material- und Geowissenschaften 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft 11 Fachbereich Material- und Geowissenschaften > Materialwissenschaft > Fachgebiet Disperse Feststoffe |
| Hinterlegungsdatum: | 22 Aug 2018 14:17 |
| Letzte Änderung: | 16 Mär 2022 13:16 |
| PPN: | |
| Sponsoren: | Office of Science, Office of Basic Energy Sciences, of the U.S. Department of Energy: DE-AC02-05CH11231, COMPRES, tConsortium for Materials Properties Research in Earth Sciences under NSF: EAR 11-57758, German Research Foundation (DFG): SPP 1415, GU 992/12-1, Advanced Light Source BL12.2.2 for beam time: DD00087 |
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